Skip to main content
. 2021 Apr 3;26(7):2052. doi: 10.3390/molecules26072052

Table 3.

Thermal properties of d-gluconic acid derived ILs.

Physical State Tm (°C) Tc (°C) Tg (°C) Td (°C) Ref.
39a Yellow viscous liquid --- --- --- >250 °C 1,2,3,4 [43]
39b Pale yellow gel --- --- --- >250 °C 1,2,3,4 [43]
39c Yellow gel --- --- --- >230 °C 1,2,3,4 [43]
39d Yellow viscous liquid --- --- --- >230 °C 1,2,3,4 [43]
40a White solid 81.5 5 --- −21.8 6; 80.2 6 155.0 7,8 [44]
40b White solid 35.6 5 73.4 5 34.0 6 161.8 7,8 [44]
40c White solid 120 5 --- 0.4 6 172.5 7,8 [44]
43 Yellow viscous oil --- --- −24.1 9 103.1 7,8 [17]
44a Light-yellow oil --- --- −0.1 9 195.1 7,8 [17]
44b Light yellow oil --- --- −19.4 9 191.7 7,8 [17]
44c Light yellow oil --- --- −7.9 9 210.3 7,8 [17]
44d Light yellow oil --- --- −46.6 9 127.8 7,8 [17]
44e Light yellow oil --- --- −55.5 9 200.6 7,8 [17]
44f Light yellow oil --- --- −36.1 9 200.6 7,8 [17]
44g Light yellow oil 87.1 8 --- −22.8 9 121.8 7,8 [17]
44h Yellow oil --- --- −16.2 9 188.5 7,8 [17]
45 Light yellow oil --- --- −3.7 9 197.3 7,8 [17]
46a Light yellow oil --- --- −16.6 10 168.4 7,8 [48]
46b Yellow oil --- --- −15.9 10 191.1 7,8 [48]

1 Determined by DSC; 2 DSC conditions: 2–8 mg of the compound; 40 °C for 10 min, then 10 °C/min to 250 °C, Crimped aluminum pan, N2 (50 mL/min); 3 The authors reported this interval of decomposition temperatures; no Td is reported for each compound; 4 Inflection point of the endothermic peak behavior; 5 DSC conditions: From −10 °C to Tmax (depending on compound stability) then cooling from Tmax to −10 °C at 10 °C/min, two heating-cooling cycles, hermetically sealed aluminum pan, N2. 6 These data have been taken from Reference [17]. For DSC conditions see note 9; 7 TGA conditions: 5 °C/min to 400–500 °C, Alumina crucibles, N2. 8 Td5% 9 DSC conditions: From −50 °C to Tmax (depending on compound stability), 10 °C/min; aluminum hermetically sealed pans, N2; 10 DSC conditions: From −20 °C to Tmax (depending on compound stability), two heating-cooling cycles, 5 °C/min, hermetically sealed aluminum pan, N2.