Table 3.
Physical State | Tm (°C) | Tc (°C) | Tg (°C) | Td (°C) | Ref. | |
---|---|---|---|---|---|---|
39a | Yellow viscous liquid | --- | --- | --- | >250 °C 1,2,3,4 | [43] |
39b | Pale yellow gel | --- | --- | --- | >250 °C 1,2,3,4 | [43] |
39c | Yellow gel | --- | --- | --- | >230 °C 1,2,3,4 | [43] |
39d | Yellow viscous liquid | --- | --- | --- | >230 °C 1,2,3,4 | [43] |
40a | White solid | 81.5 5 | --- | −21.8 6; 80.2 6 | 155.0 7,8 | [44] |
40b | White solid | 35.6 5 | 73.4 5 | 34.0 6 | 161.8 7,8 | [44] |
40c | White solid | 120 5 | --- | 0.4 6 | 172.5 7,8 | [44] |
43 | Yellow viscous oil | --- | --- | −24.1 9 | 103.1 7,8 | [17] |
44a | Light-yellow oil | --- | --- | −0.1 9 | 195.1 7,8 | [17] |
44b | Light yellow oil | --- | --- | −19.4 9 | 191.7 7,8 | [17] |
44c | Light yellow oil | --- | --- | −7.9 9 | 210.3 7,8 | [17] |
44d | Light yellow oil | --- | --- | −46.6 9 | 127.8 7,8 | [17] |
44e | Light yellow oil | --- | --- | −55.5 9 | 200.6 7,8 | [17] |
44f | Light yellow oil | --- | --- | −36.1 9 | 200.6 7,8 | [17] |
44g | Light yellow oil | 87.1 8 | --- | −22.8 9 | 121.8 7,8 | [17] |
44h | Yellow oil | --- | --- | −16.2 9 | 188.5 7,8 | [17] |
45 | Light yellow oil | --- | --- | −3.7 9 | 197.3 7,8 | [17] |
46a | Light yellow oil | --- | --- | −16.6 10 | 168.4 7,8 | [48] |
46b | Yellow oil | --- | --- | −15.9 10 | 191.1 7,8 | [48] |
1 Determined by DSC; 2 DSC conditions: 2–8 mg of the compound; 40 °C for 10 min, then 10 °C/min to 250 °C, Crimped aluminum pan, N2 (50 mL/min); 3 The authors reported this interval of decomposition temperatures; no Td is reported for each compound; 4 Inflection point of the endothermic peak behavior; 5 DSC conditions: From −10 °C to Tmax (depending on compound stability) then cooling from Tmax to −10 °C at 10 °C/min, two heating-cooling cycles, hermetically sealed aluminum pan, N2. 6 These data have been taken from Reference [17]. For DSC conditions see note 9; 7 TGA conditions: 5 °C/min to 400–500 °C, Alumina crucibles, N2. 8 Td5% 9 DSC conditions: From −50 °C to Tmax (depending on compound stability), 10 °C/min; aluminum hermetically sealed pans, N2; 10 DSC conditions: From −20 °C to Tmax (depending on compound stability), two heating-cooling cycles, 5 °C/min, hermetically sealed aluminum pan, N2.