Table 4.
Physical State | Tm(°C) | Tg(°C) | Td(°C) | Ref. | |
---|---|---|---|---|---|
52a | Solid | 142–143 1 | 2,3 (200–300) 4 | [54] | |
52a | Solid | 95 °C 1 | −20.5 5 | 136 6,7 | [55] |
52b | Oil | --- | −8.7 5 | 130 7 | [56] |
52c | Liquid | --- | --- | 2,3 (200–300, higher than 52a) 4 | [54] |
53a | Solid | 98 °C 1 | 18.3 5 | n.d.7 | [55] |
53b | Wax | --- | −22.5 5 | 142 7 | [56] |
53c | Solid | 50.1 8 | −63.3 8 | 245 9,10 | [57] |
56 | Liquid | 18.8 8 | −76.3 8 | 330 9,10 | [57] |
1 Measured on a digital melting point apparatus; 2 TGA conditions: 5–10 mg, from 25 °C to 900 °C at 10 °C/min, Al2O3 crucibles, N2 (80 mL/min) 3 No value reported, only the thermograms were depicted; 4 Approximative Td50% obtained from the reported thermograms. 5 DSC conditions: 10–20 mg, aluminum pan with a pierced lid, 10 °C/min, Ar (200 mL/min); 6 Onset temperature; 7TGA conditions: 10–20 mg of the compound, from 30 °C to 500 °C, 10 °C/min, dry Ar(50 mL/min), Alumina crucibles; 8 DSC conditions: From −100 °C to 100 °C, 2 °C/min, N2; 9 TGA conditions: From 30 °C to 450 °C, 5 °C/min, N2; 10 Decomposition temperature.