Table 6.
Physical State | Tm (°C) | Tg (°C) | Td (°C) | Ref. | |
---|---|---|---|---|---|
98b | Liquid | --- | −30 1 | 433 2,3(454) 3,4[≈400–500] 5,6,7 | [75] |
99b | Liquid | --- | −20 1 | 435 2,3(456) 3,4 | [75] |
100b | Liquid | --- | −14 1 | 446 2,3(460) 3,4 | [75] |
105a | Viscous liquid | --- | −19 8 | 198 6,9(≈300) 6.7 | [81] |
105b | Viscous liquid | --- | −18 8 | 198 6,9(≈300) 6.7 | [81] |
105c | Viscous liquid | --- | 4 8 | 208 6,9(≈300) 6.7 | [81] |
105d | Viscous liquid | --- | −15 8 | 107 6,9(≈200–300) 6.7 | [81] |
105e | Viscous liquid | --- | 6 8 | 209 6,9(≈300) 6.7 | [81] |
105f | Viscous liquid | --- | −9 8 | 207 6,9(≈300) 6.7 | [81] |
105g | Viscous liquid | --- | 0 8 | 211 6,9(≈300) 6.7 | [81] |
106b | Solid | 87–88 10 | --- | 6,11 (≈300) 6,7 | [54] |
111a | Wax | --- | 12 12 | 164 13,14(235) 2,13 | [74] |
111b | Liquid | --- | 20 12 | 208 13,14(285) 2,13 | [74] |
111c | Wax | --- | 10 12 | 191 13,14(259) 2,13 | [74] |
111d | Liquid | --- | 13 12 | 224 13,14(327) 2,13 | [74] |
111e | Wax | --- | 8 12 | 191 13,14(287) 2,13 | [74] |
112a | Solid | 121 12 | 21 12 | 178 13,14(251) 2,13 | [74] |
112b | Solid | 134 12 | --- | 202 13,14(247) 2,13 | [74] |
112c | Wax | --- | 22 12 | 201 13,14(279) 2,13 | [74] |
112d | Wax | --- | 1212 | 221 13,14(340) 2,13 | [74] |
112e | Wax | --- | 1512 | 204 13,14(296) 2,13 | [74] |
139b | Solid | 124 10 | --- | 6,11 (≈400–500, higher than 98b) 6,7 | [54] |
139c | Liquid | --- | --- | 6,11 (≈300, lower than 106b) 6,7 | [54] |
135a | Liquid | --- | --- | 225 11,15 | [99] |
135b | Solid | 66–70 10 | --- | 205 11,15 | [99] |
135c | Solid | 164–168 10 | --- | 225 11,15 | [99] |
135d | Solid | 95–100 10 | --- | 242 11,15 | [99] |
135e | Solid | 118–120 10 | --- | 215 11,15 | [99] |
137a | Solid | 60–63 10 | --- | 250 11,15 | [99] |
137b | Solid | 135–138 10 | --- | 242 11,15 | [99] |
1 DSC conditions: Heating from −65 °C to 250 °C (20 °C/min), held at 250 °C, cooling from 250 °C to −65 °C (20 °C/min), N2 (60 mL/min); 2 Td50%; 3 TGA conditions: From 25 °C to 600 °C (20 °C/min), N2 (60 mL/min); 4 Decomposition temperature; 5 These data were taken from Reference [54]; 6 TGA conditions: 5–10 mg of sample, from 25 °C to 900 °C, 10 °C/min, 70 μL Al2O3 crucibles, N2 (80 mL/min); 7 Td50% interpreted from the reported thermograms; 8 DSC conditions: From −65 °C to 150 °C, 10 °C/min, 40 μL aluminum crucibles, N2 (80 mL/min); 9 Not clearly defined; 10 Measured on a digital melting point apparatus; 11 No information on the instrumental parameters; 12 DSC conditions: 5–15 mg of the compound, heating from 25 °C to 150 °C (10 °C/min), then cooling from 150 °C to −100 °C (10 °C/min), N2, aluminum pan; 13 TGA conditions: 2–10 mg, from 30 °C to 450 °C (10 °C/min), N2; 14 Td5% (onset point at 5% weight loss); 15 Decomposition point.