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. 2021 Mar 4;84(3):724–737. doi: 10.1021/acs.jnatprod.0c01217

Table 2. 13C and 13C DEPT NMR Data of Compounds 14a.

  1 2 3 4
position δC, type δC, type δC, type δC, type
1 226.9, C 225.6, C 227.3, C 218.0, C
2 128.0, CH 130.0, CH 139.6, CH 51.0, CH
3 76.8, CH 78.1, CH 80.3, CH 78.1, CH
4 44.0, C 43.6, C 45.5, C 39.1, C
5 40.0, CH 41.1, CH 43.6, CH 41.2, CH
6 32.9, CH2 34.3, CH2 34.4, CH2 32.0, CH2
7 175.9, C 174.3, C 176.4, C 175.0, C
8 77.6, C 76.3, C 134.4, C 140.4, C
9 87.3, C 86.6, C 83.2, C 56.3, CH
10 55.5, C 54.2, C 56.4, C 50.0, C
11 28.1, CH2 29.6, CH2 29.7, CH2 20.0, CH2
12 26.3, CH2 26.2, CH2 29.7, CH2 33.8, CH2
13 38.1, C 38.7, C 39.4, C 41.0, C
14 165.8, C 165.8, C 136.4, C 44.4, CH
15 119.0, CH 119.8, CH 34.3, CH2 29.2, CH2
16 166.0, C 165.3, C 172.1, C 172.0, C
17 79.1, CH 79.4, CH 81.6, CH 77.1, CH
18 20.0, CH3 21.0, CH3 16.6, CH3 20.5, CH3
19 26.0, CH3 21.1, CH3 19.3, CH3 14.5, CH3
20 121.0, C 120.3, C 121.0, C 121.4, C
21 140.8, CH 142.6, CH 143.8, CH 141.9, CH
22 109.0, CH 110.0, CH 110.4, CH 110.0, CH
23 142.5, CH 142.2, CH 145.0, CH 141.9, CH
28 22.6, CH3 21.4, CH3 22.8, CH3 21.0, CH3
29 45.1, CH2 47.0, CH2 47.2, CH2 18.0, CH3
30 145.3, CH 145.7, CH 135.0, CH 121.7, CH
MeO-7 51.2, CH3 51.7, CH3 52.4, CH3 50.8, CH3
1′ 168.2, C 166.5, C 168.8, C 175.0, C
2′ 129.1, C 137.0, C 129.0, C 74.2, CH
3′ 141.4, CH 128.4, CH2 140.5, CH 31.1, CH
4′ 13.1, CH3 17.8, CH3 14.5, CH3 15.0, CH3
5′ 11.0, CH3   12.4, CH3 18.0, CH3
a

Spectra were recorded in methanol-d4 at 150 MHz. Chemical shifts are given in ppm; assignments were confirmed by HSQC and HMBC experiments.