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Calculated crystalline cell parameters and crystalline sizes of the Co- and Ni-containing nanopowders.
| NPs | Cell parameter a, Å | Cell volume, V, Å3 | Space group | Crystalline size d, nm |
Goodness of fit |
|---|---|---|---|---|---|
| Co | 3.53903 | 44.32532 | Fm-3m (cubic) | 11.9 | 3.53 |
| Co3Ni | 3.53186 | 44.05672 | Fm-3m (cubic) | 21.7 | 2.11 |
| CoNi | 3.53373 | 44.12663 | Fm-3m (cubic) | 27.6 | 7.06 |
| CoNi3 | 3.53118 | 44.03108 | Fm-3m (cubic) | 26.4 | 4.38 |
| Ni | 3.52711 | 43.87920 | Fm-3m (cubic) | 18.3 | 0.16 |
