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CW EPR (A) and HYSCORE (B) spectra of (3MPA/NO)-bound Av3MDO iron-nitrosyl. The instrumental parameters for (A) (previously reported) are described in detail elsewhere (12). The data in (B) were collected with the following instrumental parameters: microwave frequency, 9.78 GHz; field position of 175 mT; temperature, 5 K; pulse repetition rate, 1.25 kHz; τ, 120 ns. Additional instrumental parameters are described in detail in Experimental procedures.
