Table 3.1.
48 h stability, repeatability, recovery data, and matrix effect of samples in the ethanol-extraction.
NO. | Analytes | 48 h Stability (RSD%, n = 8) | Repeatability (RSD%, n = 6) | Recovery | (%, n = 3) | Matrix effect (%) | ||||
---|---|---|---|---|---|---|---|---|---|---|
high | middle | low | ||||||||
Mean | RSD% | Mean | RSD% | Mean | RSD% | |||||
1 | Matairesinoside | 4.33% | 3.67% | 117.84% | 2.21% | 98.57% | 4.39% | 83.14% | 3.19% | 95.85% |
2 | Arcttin | 6.98% | 1.71% | 107.08% | 0.62% | 108.86% | 1.34% | 83.68% | 3.80% | 118.49% |
3 | Matairesinol | 2.83% | 2.97% | 86.30% | 1.91% | 90.17% | 1.69% | 110.81% | 5.57% | 118.82% |
4 | Arctigenin | 1.68% | 1.57% | 87.29% | 1.40% | 92.92% | 1.09% | 98.82% | 3.25% | 119.15% |
5 | Lappaol B | 6.17% | 7.37% | – | – | – | – | – | – | 80.20% |
6 | Schisandrol A | 4.75% | 3.55% | 103.02% | 0.84% | 110.85% | 1.94% | 86.67% | 4.48% | 89.13% |
7 | Gomisin D | 5.08% | 7.48% | 92.49% | 3.68% | 95.50% | 6.37% | 109.45% | 5.78% | 80.56% |
8 | Angeloylgomisin H | 6.71% | 2.83% | 99.85% | 3.17% | 103.28% | 6.04% | 104.38% | 8.69% | 103.19% |
9 | Gomisin G | 4.78% | 2.52% | 114.49% | 2.12% | 103.46% | 7.49% | 87.81% | 8.59% | 119.95% |
10 | Schisantherin A | 2.43% | 2.99% | 88.47% | 3.67% | 88.21% | 4.21% | 91.31% | 8.35% | 109.45% |
11 | Schisantherin B | 10.45% | 0.72% | 112.47% | 3.48% | 101.71% | 4.29% | 94.84% | 4.97% | 96.26% |
12 | Schisanhenol | 1.93% | 1.48% | 93.22% | 2.11% | 90.33% | 2.46% | 98.21% | 6.63% | 118.31% |
13 | Gomisin L1 | 2.74% | 1.54% | 93.87% | 2.47% | 80.49% | 1.88% | 90.33% | 3.94% | 95.00% |
14 | Schizandrin A | 2.52% | 0.87% | 88.27% | 1.02% | 92.28% | 3.85% | 96.40% | 4.43% | 81.27% |
15 | Schizandrin B | 2.36% | 1.22% | 108.75% | 2.15% | 105.09% | 2.98% | 102.71% | 4.43% | 117.50% |
16 | Schizandrin C | 3.08% | 1.45% | 112.41% | 3.41% | 105.52% | 6.12% | 92.42% | 4.09% | 87.79% |
17 | Benzoylgomisin O | 4.86% | 2.05% | 110.19% | 4.12% | 109.80% | 6.43% | 93.18% | 3.95% | 107.48% |
18 | Angeloylgomisin O | 8.21% | 3.95% | 120.11% | 1.89% | 105.34% | 2.63% | 89.44% | 5.27% | 87.95% |