Table 3.2.
NO. | Analytes | 48 h Stability (RSD%, n = 8) | Repeatability (RSD%, n = 6) | Recovery | (%, n = 3) | Matrix effect (%) | ||||
---|---|---|---|---|---|---|---|---|---|---|
high | middle | low | ||||||||
Mean | RSD% | Mean | RSD% | Mean | RSD% | |||||
1 | Matairesinoside | 4.60% | 2.25% | 119.28% | 0.90% | 114.91% | 5.39% | 84.57% | 6.06% | 96.66% |
2 | Arcttin | 3.81% | 3.03% | 102.11% | 5.14% | 101.47% | 5.57% | 87.08% | 9.51% | 92.29% |
3 | Matairesinol | 1.56% | 1.15% | 83.31% | 7.54% | 88.12% | 3.92% | 94.59% | 3.49% | 89.11% |
4 | Arctigenin | 1.76% | 0.51% | 82.63% | 4.52% | 95.75% | 2.87% | 90.98% | 10.40% | 88.04% |
5 | Lappaol B | 9.89% | 4.62% | 84.94% | 4.75% | 118.61% | 2.84% | 119.25% | 2.20% | 114.62% |
6 | Schisandrol A | 6.12% | 1.64% | 92.28% | 4.81% | 116.42% | 1.59% | 111.13% | 3.98% | 85.74% |
7 | Gomisin D | 5.41% | 2.38% | 102.05% | 2.32% | 99.45% | 3.58% | 115.05% | 1.96% | 97.76% |
8 | Angeloylgomisin H | 2.74% | 1.90% | 86.67% | 2.78% | 94.35% | 6.25% | 111.25% | 4.01% | 112.33% |
9 | Gomisin G | 4.23% | 1.55% | 89.10% | 4.53% | 105.32% | 2.39% | 83.81% | 2.68% | 81.65% |
10 | Schisantherin A | 5.42% | 4.30% | 83.35% | 5.95% | 106.05% | 3.81% | 83.12% | 1.20% | 83.14% |
11 | Schisantherin B | 2.31% | 2.23% | 89.03% | 4.39% | 89.42% | 5.82% | 114.34% | 2.18% | 81.33% |
12 | Schisanhenol | 2.64% | 1.89% | 81.09% | 1.01% | 86.30% | 5.44% | 87.34% | 8.41% | 82.35% |
13 | Gomisin L1 | 2.36% | 4.09% | 92.91% | 2.38% | 118.16% | 2.02% | 98.30% | 1.18% | 102.44% |
14 | Schizandrin A | 4.40% | 5.88% | 89.76% | 3.89% | 92.00% | 6.76% | 82.64% | 1.17% | 110.83% |
15 | Schizandrin B | 4.66% | 1.60% | 96.65% | 3.65% | 103.43% | 3.01% | 117.43% | 1.68% | 88.12% |
16 | Schizandrin C | 2.66% | 2.25% | 90.73% | 6.76% | 97.84% | 3.32% | 83.52% | 2.63% | 102.25% |
17 | Benzoylgomisin O | 4.06% | 4.79% | 98.34% | 4.81% | 96.15% | 5.61% | 115.32% | 0.38% | 101.36% |
18 | Angeloylgomisin O | 3.35% | 4.02% | 82.44% | 3.45% | 89.20% | 4.54% | 101.46% | 8.32% | 98.87% |