| Crystal data |
| Chemical formula |
[Ir(C11H8N)2Cl(C25H22P2)] |
|
M
r
|
920.38 |
| Crystal system, space group |
Monoclinic, P21/n
|
| Temperature (K) |
293 |
|
a, b, c (Å) |
14.4506 (5), 15.4490 (5), 17.8532 (6) |
| β (°) |
103.044 (1) |
|
V (Å3) |
3882.8 (2) |
|
Z
|
4 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
3.63 |
| Crystal size (mm) |
0.19 × 0.09 × 0.06 |
| |
| Data collection |
| Diffractometer |
Bruker APEX CCD area-detector |
| Absorption correction |
Multi-scan (SADABS; Bruker, 2003 ▸) |
|
T
min, T
max
|
0.800, 1.000 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
35153, 9248, 7758 |
|
R
int
|
0.033 |
| (sin θ/λ)max (Å−1) |
0.658 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.026, 0.062, 1.05 |
| No. of reflections |
9248 |
| No. of parameters |
478 |
| H-atom treatment |
H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) |
0.90, −0.33 |
