| Bruker SMART APEXII CCD diffractometer | 5291 independent reflections |
| Radiation source: sealed tube | 4023 reflections with I > 2σ(I) |
| Detector resolution: 8.333 pixels mm-1 | Rint = 0.041 |
| φ and ω scans | θmax = 31.1°, θmin = 2.7° |
| Absorption correction: multi-scan (SADABS; Sheldrick, 2008) | h = −21→21 |
| Tmin = 0.885, Tmax = 0.975 | k = −12→12 |
| 21434 measured reflections | l = −18→18 |