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. 2021 Feb 26;77(Pt 3):314–318. doi: 10.1107/S2056989021001778
Bruker SMART APEXII CCD diffractometer 5291 independent reflections
Radiation source: sealed tube 4023 reflections with I > 2σ(I)
Detector resolution: 8.333 pixels mm-1 Rint = 0.041
φ and ω scans θmax = 31.1°, θmin = 2.7°
Absorption correction: multi-scan (SADABS; Sheldrick, 2008) h = −21→21
Tmin = 0.885, Tmax = 0.975 k = −12→12
21434 measured reflections l = −18→18