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. 2021 Feb 5;77(Pt 3):226–232. doi: 10.1107/S2056989021001183
N1—C7 1.391 (2) C9—C17 1.542 (2)
N1—C18 1.465 (2) C10—C11 1.381 (3)
N1—C5 1.467 (2) C10—H10 0.9300
C1—C2 1.514 (3) C11—C12 1.381 (3)
C1—C6 1.533 (2) C11—H11 0.9300
C1—H1A 0.9700 C12—C13 1.388 (3)
C1—H1B 0.9700 C12—C15 1.512 (3)
C2—C3 1.511 (3) C13—H13 0.9300
C2—H2A 0.9700 C14—H14A 0.9600
C2—H2B 0.9700 C14—H14B 0.9600
C3—C14 1.517 (3) C14—H14C 0.9600
C3—C4 1.525 (2) C15—H15A 0.9600
C3—H3 0.9800 C15—H15B 0.9600
C4—C5 1.530 (2) C15—H15C 0.9600
C4—H4A 0.9700 C16—H16A 0.9600
C4—H4B 0.9700 C16—H16B 0.9600
C5—C6 1.532 (2) C16—H16C 0.9600
C5—H5 0.9800 C17—H17A 0.9600
C6—C9 1.550 (2) C17—H17B 0.9600
C6—H6 0.9800 C17—H17C 0.9600
C7—C10 1.404 (2) C18—C19 1.469 (3)
C7—C8 1.407 (2) C18—H18A 0.9700
C8—C13 1.392 (2) C18—H18B 0.9700
C8—C9 1.528 (2) C19—C20 1.168 (3)
C9—C16 1.539 (2) C20—H20 0.9300
C7—N1—C18 117.18 (14) C8—C9—C6 108.94 (13)
C7—N1—C5 121.04 (13) C16—C9—C6 112.13 (14)
C18—N1—C5 117.14 (14) C17—C9—C6 108.53 (13)
C2—C1—C6 112.89 (15) C11—C10—C7 121.85 (16)
C2—C1—H1A 109.0 C11—C10—H10 119.1
C6—C1—H1A 109.0 C7—C10—H10 119.1
C2—C1—H1B 109.0 C10—C11—C12 121.23 (17)
C6—C1—H1B 109.0 C10—C11—H11 119.4
H1A—C1—H1B 107.8 C12—C11—H11 119.4
C3—C2—C1 111.02 (17) C11—C12—C13 116.75 (17)
C3—C2—H2A 109.4 C11—C12—C15 121.55 (18)
C1—C2—H2A 109.4 C13—C12—C15 121.69 (18)
C3—C2—H2B 109.4 C12—C13—C8 124.06 (16)
C1—C2—H2B 109.4 C12—C13—H13 118.0
H2A—C2—H2B 108.0 C8—C13—H13 118.0
C2—C3—C14 112.77 (19) C3—C14—H14A 109.5
C2—C3—C4 109.82 (15) C3—C14—H14B 109.5
C14—C3—C4 111.95 (16) H14A—C14—H14B 109.5
C2—C3—H3 107.3 C3—C14—H14C 109.5
C14—C3—H3 107.3 H14A—C14—H14C 109.5
C4—C3—H3 107.3 H14B—C14—H14C 109.5
C3—C4—C5 113.42 (14) C12—C15—H15A 109.5
C3—C4—H4A 108.9 C12—C15—H15B 109.5
C5—C4—H4A 108.9 H15A—C15—H15B 109.5
C3—C4—H4B 108.9 C12—C15—H15C 109.5
C5—C4—H4B 108.9 H15A—C15—H15C 109.5
H4A—C4—H4B 107.7 H15B—C15—H15C 109.5
N1—C5—C4 110.99 (13) C9—C16—H16A 109.5
N1—C5—C6 110.04 (13) C9—C16—H16B 109.5
C4—C5—C6 109.98 (13) H16A—C16—H16B 109.5
N1—C5—H5 108.6 C9—C16—H16C 109.5
C4—C5—H5 108.6 H16A—C16—H16C 109.5
C6—C5—H5 108.6 H16B—C16—H16C 109.5
C5—C6—C1 109.31 (14) C9—C17—H17A 109.5
C5—C6—C9 113.23 (13) C9—C17—H17B 109.5
C1—C6—C9 113.91 (13) H17A—C17—H17B 109.5
C5—C6—H6 106.6 C9—C17—H17C 109.5
C1—C6—H6 106.6 H17A—C17—H17C 109.5
C9—C6—H6 106.6 H17B—C17—H17C 109.5
N1—C7—C10 120.02 (14) N1—C18—C19 112.97 (15)
N1—C7—C8 122.17 (14) N1—C18—H18A 109.0
C10—C7—C8 117.80 (15) C19—C18—H18A 109.0
C13—C8—C7 118.29 (15) N1—C18—H18B 109.0
C13—C8—C9 120.52 (14) C19—C18—H18B 109.0
C7—C8—C9 121.15 (15) H18A—C18—H18B 107.8
C8—C9—C16 108.30 (13) C20—C19—C18 178.9 (2)
C8—C9—C17 110.19 (14) C19—C20—H20 180.0
C16—C9—C17 108.76 (15)
C6—C1—C2—C3 −57.2 (2) C10—C7—C8—C9 178.42 (14)
C1—C2—C3—C14 −179.78 (16) C13—C8—C9—C16 78.32 (19)
C1—C2—C3—C4 54.6 (2) C7—C8—C9—C16 −99.15 (18)
C2—C3—C4—C5 −55.6 (2) C13—C8—C9—C17 −40.5 (2)
C14—C3—C4—C5 178.33 (16) C7—C8—C9—C17 142.00 (16)
C7—N1—C5—C4 −155.23 (15) C13—C8—C9—C6 −159.48 (14)
C18—N1—C5—C4 49.6 (2) C7—C8—C9—C6 23.05 (19)
C7—N1—C5—C6 −33.3 (2) C5—C6—C9—C8 −48.98 (16)
C18—N1—C5—C6 171.56 (14) C1—C6—C9—C8 −174.71 (13)
C3—C4—C5—N1 178.18 (14) C5—C6—C9—C16 70.87 (17)
C3—C4—C5—C6 56.18 (18) C1—C6—C9—C16 −54.85 (19)
N1—C5—C6—C1 −177.26 (14) C5—C6—C9—C17 −168.97 (13)
C4—C5—C6—C1 −54.69 (17) C1—C6—C9—C17 65.30 (18)
N1—C5—C6—C9 54.59 (17) N1—C7—C10—C11 179.08 (18)
C4—C5—C6—C9 177.16 (12) C8—C7—C10—C11 −1.8 (3)
C2—C1—C6—C5 56.8 (2) C7—C10—C11—C12 1.3 (3)
C2—C1—C6—C9 −175.44 (15) C10—C11—C12—C13 0.1 (3)
C18—N1—C7—C10 −18.0 (2) C10—C11—C12—C15 −178.6 (2)
C5—N1—C7—C10 −173.17 (15) C11—C12—C13—C8 −1.0 (3)
C18—N1—C7—C8 162.92 (16) C15—C12—C13—C8 177.72 (19)
C5—N1—C7—C8 7.7 (2) C7—C8—C13—C12 0.5 (3)
N1—C7—C8—C13 180.00 (15) C9—C8—C13—C12 −177.06 (15)
C10—C7—C8—C13 0.9 (2) C7—N1—C18—C19 86.5 (2)
N1—C7—C8—C9 −2.5 (2) C5—N1—C18—C19 −117.36 (18)