| Crystal data |
| Chemical formula |
[Cu(C4H4O6)(C10H8N2)] |
|
M
r
|
367.80 |
| Crystal system, space group |
Triclinic, P\overline{1} |
| Temperature (K) |
90 |
|
a, b, c (Å) |
7.6516 (5), 9.9272 (6), 10.0722 (6) |
| α, β, γ (°) |
95.204 (4), 107.729 (4), 111.462 (4) |
|
V (Å3) |
660.34 (7) |
|
Z
|
2 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
1.69 |
| Crystal size (mm) |
0.15 × 0.09 × 0.07 |
| |
| Data collection |
| Diffractometer |
Bruker Kappa APEXII DUO CCD |
| Absorption correction |
Multi-scan (SADABS; Krause et al., 2015 ▸) |
|
T
min, T
max
|
0.838, 0.891 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
18442, 4041, 2675 |
|
R
int
|
0.063 |
| (sin θ/λ)max (Å−1) |
0.715 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.049, 0.105, 1.02 |
| No. of reflections |
4041 |
| No. of parameters |
214 |
| No. of restraints |
2 |
| H-atom treatment |
H atoms treated by a mixture of independent and constrained refinement |
| Δρmax, Δρmin (e Å−3) |
0.74, −0.56 |
