| Bruker D8 VENTURE PHOTON 100 CMOS diffractometer | 3665 independent reflections |
| Radiation source: INCOATEC IµS micro–focus source | 3140 reflections with I > 2σ(I) |
| Mirror monochromator | Rint = 0.031 |
| Detector resolution: 10.4167 pixels mm-1 | θmax = 74.6°, θmin = 4.3° |
| ω scans | h = −17→16 |
| Absorption correction: multi-scan (SADABS; Krause et al., 2015) | k = −19→18 |
| Tmin = 0.86, Tmax = 0.95 | l = −10→9 |
| 13875 measured reflections |