| Bruker D8 VENTURE PHOTON 100 CMOS diffractometer | 3372 independent reflections |
| Radiation source: INCOATEC IµS micro–focus source | 2939 reflections with I > 2σ(I) |
| Mirror monochromator | Rint = 0.031 |
| Detector resolution: 10.4167 pixels mm-1 | θmax = 74.5°, θmin = 3.3° |
| ω scans | h = −14→16 |
| Absorption correction: multi-scan (SADABS; Krause et al., 2015) | k = −18→19 |
| Tmin = 0.88, Tmax = 0.95 | l = −9→9 |
| 13222 measured reflections |