| Time, min | 1% Acetic Acid, (%) | Methanol, (%) |
| 0 | 90.0 | 10.0 |
| 36 | 78.0 | 22.0 |
| 37 | 70.0 | 30.0 |
| 47 | 60.0 | 40.0 |
| 58 | 54.0 | 46.0 |
| 59 | 40.0 | 60.0 |
| 71 | 20.0 | 80.0 |
| 72 | 90.0 | 10.0 |
| 75 | 90.0 | 10.0 |
| Time, min | 1% Acetic Acid, (%) | Methanol, (%) |
| 0 | 90.0 | 10.0 |
| 36 | 78.0 | 22.0 |
| 37 | 70.0 | 30.0 |
| 47 | 60.0 | 40.0 |
| 58 | 54.0 | 46.0 |
| 59 | 40.0 | 60.0 |
| 71 | 20.0 | 80.0 |
| 72 | 90.0 | 10.0 |
| 75 | 90.0 | 10.0 |