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13C CPMAS NMR spectra of (a) MIL-100(Al) and MIL-100(Al) loaded with (b) 8.3 wt.% DOX, (c) 14.8 wt.% DOX and (d) 27.4 wt.% DOX. In (f) is shown the 13C NMR spectrum of DOX in the solid-state and in (e) a simulation of the liquid-state NMR spectrum.
