TABLE 2.
13C NMR (150 MHz) data of 2–10 in DMSO-d6.
| No. | 2 | 3 | 4 | 5 | 6 | 7 | 8 | 9 | 10 |
| 1 | 71.4 | 71.3 | 71.7 | 71.9 | 72.2 | 75.1 | 75.4 | 74.9 | 75.6 |
| 2 | 32.2 | 31.9 | 32.1 | 32.1 | 32.0 | 71.5 | 71.7 | 71.3 | 71.7 |
| 3 | 119.0 | 122.6 | 118.2 | 117.3 | 116.9 | 126.8 | 123.4 | 126.0 | 122.8 |
| 4 | 143.3 | 141.4 | 143.9 | 148.7 | 149.3 | 141.4 | 142.5 | 140.4 | 143.1 |
| 5 | 44.3 | 43.2 | 43.9 | 44.3 | 43.8 | 45.5 | 46.3 | 45.3 | 46.0 |
| 6 | 68.9 | 75.3 | 71.9 | 69.1 | 72.2 | 72.4 | 69.2 | 75.5 | 72.2 |
| 7 | 75.6 | 72.4 | 73.7 | 75.6 | 73.7 | 73.2 | 75.4 | 72.0 | 73.5 |
| 8 | 80.3 | 81.1 | 80.8 | 80.3 | 80.7 | 80.6 | 80.6 | 81.5 | 81.2 |
| 9 | 38.2 | 37.9 | 37.9 | 38.2 | 37.9 | 37.9 | 37.8 | 37.5 | 37.5 |
| 10 | 42.5 | 42.9 | 42.5 | 42.6 | 42.6 | 41.1 | 41.3 | 41.4 | 41.2 |
| 11 | 28.3 | 28.5 | 28.6 | 28.2 | 28.6 | 28.1 | 28.3 | 28.6 | 28.6 |
| 12 | 27.3 | 27.9 | 27.8 | 27.3 | 27.8 | 27.5 | 27.2 | 27.9 | 27.7 |
| 13 | 76.5 | 76.2 | 76.2 | 76.5 | 76.2 | 76.5 | 76.5 | 76.3 | 76.2 |
| 14 | 43.4 | 43.2 | 43.4 | 43.4 | 43.4 | 43.1 | 43.2 | 43.1 | 43.2 |
| 15 | 174.4 | 174.2 | 174.4 | 174.3 | 174.4 | 174.0 | 174.4 | 174.3 | 174.5 |
| 16 | 76.2 | 75.8 | 76.2 | 76.2 | 76.2 | 76.0 | 76.3 | 76.0 | 76.4 |
| 17 | 19.5 | 19.5 | 19.8 | 19.6 | 19.9 | 18.4 | 18.9 | 19.0 | 19.2 |
| 18 | 64.1 | 63.7 | 64.2 | 61.7 | 62.0 | 19.4 | 63.4 | 62.5 | 63.6 |
| 19 | 15.9 | 16.8 | 15.8 | 16.1 | 16.1 | 17.2 | 16.8 | 17.6 | 16.7 |
| 20 | 20.8 | 20.7 | 21.0 | 21.0 | 21.1 | 20.6 | 20.8 | 20.8 | 20.9 |
| 1’ | 164.0 | 164.0 | 164.1 | 164.1 | 164.1 | 164.2 | 164.3 | 164.3 | 164.3 |
| 2’ | 125.6 | 125.6 | 125.6 | 125.7 | 125.7 | 125.9 | 125.9 | 126.3 | 126.0 |
| 3’ | 149.9 | 150.0 | 150.0 | 150.0 | 150.0 | 150.2 | 150.2 | 150.3 | 150.2 |
| 5’ | 153.8 | 153.8 | 153.8 | 153.9 | 153.8 | 153.8 | 153.8 | 153.9 | 153.8 |
| 6’ | 124.2 | 124.2 | 124.1 | 124.1 | 124.1 | 124.1 | 124.2 | 124.2 | 124.1 |
| 7’ | 137.0 | 137.1 | 137.0 | 137.0 | 136.9 | 137.1 | 137.1 | 137.1 | 137.1 |
| 1” | 170.0 | 169.6 | 170.2 | ||||||
| 2” | 21.4 | 21.1 | 21.5 | ||||||
| 1”’ | 170.7 | 170.6 | 170.3 | 170.7 | |||||
| 2”’ | 21.1 | 21.0 | 20.6 | 21.1 | |||||
| 1”” | 170.0 | 170.0 | 170.0 | 170.0 | 170.1 | 170.0 | |||
| 2”” | 20.9 | 20.8 | 20.9 | 20.9 | 20.7 | 20.9 |