Table B.1.

DELOS process parameters kept constant in all DoE experimental runs.

Process Parameter	Value	Control
Working temperature, Tw	35 °C	Heating jacket
High pressure stirring	500 rpm	Magnetic stirrer controller
Working pressure, Pw	9 MPa	Syringe pump for CO2
Depressurization pressure in the autoclave	10 MPa	Manometer and N2 pressure regulator
Collector Stirring	300 rpm	Plate with magnetic stirrer
CO2 molar fraction, XCO2	0.55	Solvent volume in the reactor
Depressurization flowrate	10 g/min	Manually controlled due to scale, averaged
Collector temperature	23 °C	Monitored, room temperature