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. 2021 Apr 13;8(Pt 3):444–454. doi: 10.1107/S2052252521002852

Table 3. Details of the PDF measurements for thin-film samples.

Film sample Measurement Temperature profile Environment
ZSA1_423K (p2) Ex situ GI-PDF RT, 483 K, 553 K, 573 K_1 h, 573 K_2 h; heating rate: 2 K min−1 Air
   
ZSA2 (s2) In situ GI-PDF 300\,{\rm K}\mathop \to \limits^{{\rm{5\,K\,min}}^{-1}}573\,{\rm K}\mathop \to \limits^{{\rm dwell}}573\,{\rm K}\mathop \to \limits^{{\rm{naturally\,cooling}}}{\rm RT} Air
ZSA3 (s2)
   
ZS2 (s2) In situ NI-PDF with resistivity 423\,{\rm K}\mathop \to \limits^{{\rm 1\,K\,min}^{-1}}603\,{\rm K}\mathop \to \limits^{\rm naturally\,cooling}{\rm RT} Air
ZS3_373K