Skip to main content
. Author manuscript; available in PMC: 2021 May 3.
Published in final edited form as: J Am Chem Soc. 2017 Sep 26;139(40):14302–14314. doi: 10.1021/jacs.7b08640

Figure 1.

Figure 1.

a) HPLC chromatogram of the phen chlorido species 5 (blue, top trace) and the corresponding aqua species 12 (red, bottom trace) using a methanol gradient elution and monitoring 260 nm. b) 1H NMR spectra of the phen aqua species 12 in MeOD-d4 (blue, top trace) and in MeOD-d4 with 15% D2O (red, bottom trace). The circles designate peaks due to the aqua complex and the x’s designate peaks due to the methanol adduct.