Table 1. Data-collection statistics for Fab complexes.
PDZ tandem | 181-PA14-184 | 235-PA14-236 |
---|---|---|
Space group | P212121 | P21 |
a, b, c (Å) | 52.36, 75.20, 172.53 | 81.36, 80.18, 168.54 |
α, β, γ (°) | 90, 90, 90 | 90, 95.7, 90 |
No. of complexes in asymmetric unit | 1 | 2 |
X-ray source | BL-5A, PF | BL-17A, PF |
Wavelength (Å) | 1.0000 | 0.9800 |
Resolution limits (Å) | 45.68–2.50 (2.60–2.50) | 38.99–3.20 (3.36–3.20) |
No. of unique reflections | 24452 (2685) | 35827 (4745) |
Completeness (%) | 99.9 (99.6) | 99.5 (99.7) |
Multiplicity | 6.6 (6.8) | 3.4 (3.5) |
〈I/σ(I)〉 | 13.1 (1.5) | 8.0 (1.2) |
R merge | 0.093 (1.469) | 0.115 (0.965) |
R meas | 0.102 (1.589) | 0.137 (1.141) |
CC1/2 | 0.998 (0.674) | 0.994 (0.774) |