| Crystal data |
| Chemical formula |
C17H26N2O |
C17H27N2O+·0.5C4H2O4
2−
|
|
M
r
|
274.40 |
332.43 |
| Crystal system, space group |
Monoclinic, P21/n
|
Triclinic, P\overline{1} |
| Temperature (K) |
297 |
297 |
|
a, b, c (Å) |
6.2223 (3), 13.0931 (6), 19.7791 (10) |
9.2956 (6), 9.4443 (6), 12.7427 (8) |
| α, β, γ (°) |
90, 91.825 (2), 90 |
78.552 (2), 75.929 (2), 60.806 (2) |
|
V (Å3) |
1610.57 (13) |
943.06 (11) |
|
Z
|
4 |
2 |
| Radiation type |
Mo Kα |
Mo Kα |
| μ (mm−1) |
0.07 |
0.08 |
| Crystal size (mm) |
0.38 × 0.3 × 0.06 |
0.3 × 0.22 × 0.2 |
| |
| Data collection |
| Diffractometer |
Bruker D8 Venture CMOS |
Bruker D8 Venture CMOS |
| Absorption correction |
Multi-scan (SADABS; Bruker, 2018 ▸) |
Multi-scan (SADABS; Bruker, 2018 ▸) |
|
T
min, T
max
|
0.687, 0.745 |
0.722, 0.745 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
29365, 3035, 2466 |
37231, 3565, 3006 |
|
R
int
|
0.038 |
0.032 |
| (sin θ/λ)max (Å−1) |
0.610 |
0.611 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.042, 0.117, 1.06 |
0.052, 0.142, 1.05 |
| No. of reflections |
3035 |
3565 |
| No. of parameters |
189 |
228 |
| H-atom treatment |
H atoms treated by a mixture of independent and constrained refinement |
H atoms treated by a mixture of independent and constrained refinement |
| Δρmax, Δρmin (e Å−3) |
0.14, −0.17 |
0.29, −0.15 |
