Table 3. Experimental details.
| Crystal data | |
| Chemical formula | C17H13NO3 |
| M r | 279.28 |
| Crystal system, space group | Monoclinic, C2/c |
| Temperature (K) | 293 |
| a, b, c (Å) | 20.3883 (6), 7.5925 (2), 17.9858 (5) |
| β (°) | 95.791 (1) |
| V (Å3) | 2769.96 (13) |
| Z | 8 |
| Radiation type | Mo Kα |
| μ (mm−1) | 0.09 |
| Crystal size (mm) | 0.32 × 0.23 × 0.10 |
| Data collection | |
| Diffractometer | Bruker APEXII CCD |
| Absorption correction | Multi-scan (SADABS; Bruker, 2009 ▸) |
| T min, T max | 0.98, 0.99 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 35544, 2495, 1548 |
| R int | 0.12 |
| (sin θ/λ)max (Å−1) | 0.600 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.057, 0.101, 1.00 |
| No. of reflections | 2495 |
| No. of parameters | 190 |
| H-atom treatment | H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) | 0.09, −0.16 |