Table 1.
Data collection statistics.
| Data collection | MicroEDa,b | SFXc |
|---|---|---|
| Temperature (K) | 77 | 300 |
| Space group | C2 | C2 |
| Cell dimensions | ||
| a, b, c (Å) | 99.06, 31.01, 54.30 | 100.40, 31.50. 54.50 |
| α, β, γ (°) | 90.00, 107.70, 90.00 | 90.00, 107.40, 90.00 |
| Resolution (Å) | 30.54–3.00 (3.11–3.00) | 30.93–2.30 (2.38–2.30) |
| Rmerge | 0.46 (0.95) | - |
| Rsplit | - | 0.34 (1.3) |
| Mean I/σ(I) | 4.8 (1.8) | 2.6 (1.4) |
| CC1/2 | 0.95 (0.43) | 0.90 (0.36) |
| CC* | 0.99 (0.77) | 0.97 (0.73) |
| Completeness (%) | 73.7 (57.3) | 91.4 (60.2) |
| Multiplicity | 12.2 (6.0) | 24.2 (3.4) |
Values in parentheses are for the highest-resolution shell. Intensity statistics were generated from phenix.table_one98 for the MicroED data and from CrystFel107,128 for the SFX data.
aMerged data from 18 crystals.
bMicroED data were truncated at mean I/σ(I) ≥ 1.5 and CC1/2 ≥ 0.494.
cMerged data from 4725 indexed snapshots out of 13,528 hits.