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. 2021 May 13;11:10195. doi: 10.1038/s41598-021-89376-0

Table 2.

In vitro time-dependent antiproliferative effect, expressed as concentration required to induce total cell growth inhibition (TGI, μg/mL), of doxorubicin (positive control), free bromelain solution, chitosan-bromelain nanoparticles (C-B-NP), and chitosan nanoparticles (C-NP).

Cell linesb TGIa
U251 HaCaT
48c 144c 48c 144c
Doxorubicind 0.26 ± 0.09 0.09 ± 0.08 0.09 ± 0.01 0.11 ± 0.06
Bromelaind > 250 0.25 > 250 119.3 ± 21.4
C-B-NPd > 250 0.25 > 250 > 250
C-NPd > 250 > 250 > 250 > 250

aResults expressed as total growth inhibition (in μg/mL) followed by standard error, calculated by sigmoidal regression using Origin 8.0 software.

bHuman tumor cell lines: U251, glioblastoma; Human non-tumor cell line: HaCaT, immortalized keratinocytes.

cTime exposure: 48 h and 144 h.

dSamples: doxorubicin (chemotherapeutic drug; 0.025–25 μg/mL); Bromelain (0.025–25 μg/mL, considering protein concentration); chitosan-bromelain nanoparticles (0.025–25 μg/mL, considering equivalent protein concentration of free bromelain); chitosan nanoparticles (0.025–25 μg/mL, considering equivalent amount of chitosan-bromelain nanoparticles).