Table 2.
Limits of detection (LOD), limits of quantification (LOQ), upper limits of quantification (ULOQ), percent recovery, matrix effect ratio, type of regression used for the calibration curve, and representative regression equations of targeted compounds.
Compound | LOD (ng/mL) | LOQ (ng/mL) | ULOQ (ng/mL) | % Recovery | Matrix effect ratio | Calibration curve regression utilized | Representative regression equation |
---|---|---|---|---|---|---|---|
α-TP | 0.008 | 0.025 | 10,000 | 44 | 0.42 | Linear | 0.0038x + 0.0084 |
γ-TP | 0.333 | 1.11 | 1,000 | 41 | 0.22 | Linear | 1.37e−4x + 2.87e−5 |
α-TT | 0.029 | 0.095 | 1,000 | 44 | 0.36 | Linear | 0.0047x + 4.4e−5 |
γ-TT | 0.125 | 0.417 | 1,000 | 42 | 0.35 | Linear | 0.002x − 4.21e−4 |
α-CMBHC | 0.010 | 0.032 | 1,000 | 66 | 0.42 | Quadratic | −2.1e−5x2 + 0.069x + 0.270 |
α-CEHC | 0.022 | 0.074 | 1,000 | 93 | 0.54 | Quadratic | −1.2e−5x2 + 0.054x + 0.130 |
γ-CEHC | 0.026 | 0.087 | 1,000 | 96 | 0.53 | Quadratic | −3.9e−6x2 + 0.016x + 0.056 |