Table 2.
Compound | LOD (ng/mL) | LOQ (ng/mL) | ULOQ (ng/mL) | % Recovery | Matrix effect ratio | Calibration curve regression utilized | Representative regression equation |
---|---|---|---|---|---|---|---|
α-TP | 0.008 | 0.025 | 10,000 | 44 | 0.42 | Linear | 0.0038x + 0.0084 |
γ-TP | 0.333 | 1.11 | 1,000 | 41 | 0.22 | Linear | 1.37e−4x + 2.87e−5 |
α-TT | 0.029 | 0.095 | 1,000 | 44 | 0.36 | Linear | 0.0047x + 4.4e−5 |
γ-TT | 0.125 | 0.417 | 1,000 | 42 | 0.35 | Linear | 0.002x − 4.21e−4 |
α-CMBHC | 0.010 | 0.032 | 1,000 | 66 | 0.42 | Quadratic | −2.1e−5x2 + 0.069x + 0.270 |
α-CEHC | 0.022 | 0.074 | 1,000 | 93 | 0.54 | Quadratic | −1.2e−5x2 + 0.054x + 0.130 |
γ-CEHC | 0.026 | 0.087 | 1,000 | 96 | 0.53 | Quadratic | −3.9e−6x2 + 0.016x + 0.056 |