Optimization of the PEGylation of 5,10,15,20-tetrakis(pentafluorophenyl)porphyrin with 2-(2-aminoethoxy)ethanol carried out in NMP.

Entry	Equiv. amine-PEG	Reaction conditions	Yield (%)
1	10	MW, 200 °C, 2 min	9
2	10	MW, 200 °C, 5 min	42
3	20	MW, 200 °C, 5 min	45
4	10	MW, 70 °C, 18 min	48
5	10	MW, 200 °C, 10 min	77
6	10	200 °C, 3 h	68