Table 1.
X-ray crystallography data collection parameters and structure refinement statistics.
| Data collection | |
|---|---|
| Beamline | I03 at Diamond |
| Space group | H 3 2 |
| Cell parameters a, b, c (Å) | 203.6, 203.6, 99.0 |
| Resolution range (Å) | 65.83–2.18 (2.24–2.18) |
| Unique reflections | 40642 (2830) |
| Rsymm (%) | 7 (53) |
| Completeness (%) | 100 (100) |
| I/σ(I) | 23.5 (4.4) |
| Average Mosaicity (°) | 0.5 |
| B-factor from Wilson Plot (Å2) | 44.8 |
| Monomers/AU | 2 |
| Solvent content (%) | 52.2 |
| Matthews coeff. (Å3/Da) | 2.6 |
| Refinement | |
| Resolution range (Å) | 2.18–65.83 |
| Reflections (cross-validation) | 2036 (5%) |
| Rfactor/Rfree (%) | 17.8/20.3 |
| Rmsd from standard geometry | |
| Bond length (Å) | 0.012 |
| Bond angles (°) | 1.435 |
| Ramachandran plot | |
| Most favored (%) | 96 |
| Allowed (%) | 4 |
| Outlier (%) | 0 |