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. 2019 Nov 11;11(1):257–263. doi: 10.1039/c9sc04820k

Preparation of the organozinc halides.

graphic file with name c9sc04820k-u1.jpg
Entry RX 1 Time % conva Titerb
1 PhI 1a 2 h 99 0.89 M
2 4-MeO2CC6H4I 1b 2 h 99 0.90 M
3 c-HexBr 1c 22 h 97 0.86 M
4 n-C8H17Br 1d 4 h 98 0.87 M
5 4-CF3C6H4I 1e 2 h 99 0.95 M
a

Apparent conversion determined by GC analysis after hydrolysis of the reaction mixture.

b

Determined by GC analysis after iodolysis of the reaction mixture.17