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. 2021 May 20;16(5):e0251009. doi: 10.1371/journal.pone.0251009

Table 3. XRD results for 17 sample HAp.

Run A B C Responses
Temperature (°C) Time (h) pH Crystal size Crystallinity (%)
1 100 4 4 60.23 55.83
2 160 10 10 45.48 86.13
3 70 7 7 28.76 68.86
4 130 7 13 46.81 72.92
5 160 4 4 84.10 58.07
6 130 7 1 - -
7 100 10 4 65.15 57.50
8 160 4 10 38.98 82.53
9 130 7 7 45.82 76.85
10 130 7 7 46.88 77.89
11 130 1 7 44.10 75.16
12 160 10 4 89.00 59.14
13 100 10 10 31.59 78.88
14 130 13 7 56.18 80.01
15 100 4 10 29.18 74.82
16 190 7 7 71.15 79.84
17 130 7 7 44.77 74.82