Table 3. XRD results for 17 sample HAp.
Run | A | B | C | Responses | |
---|---|---|---|---|---|
Temperature (°C) | Time (h) | pH | Crystal size | Crystallinity (%) | |
1 | 100 | 4 | 4 | 60.23 | 55.83 |
2 | 160 | 10 | 10 | 45.48 | 86.13 |
3 | 70 | 7 | 7 | 28.76 | 68.86 |
4 | 130 | 7 | 13 | 46.81 | 72.92 |
5 | 160 | 4 | 4 | 84.10 | 58.07 |
6 | 130 | 7 | 1 | - | - |
7 | 100 | 10 | 4 | 65.15 | 57.50 |
8 | 160 | 4 | 10 | 38.98 | 82.53 |
9 | 130 | 7 | 7 | 45.82 | 76.85 |
10 | 130 | 7 | 7 | 46.88 | 77.89 |
11 | 130 | 1 | 7 | 44.10 | 75.16 |
12 | 160 | 10 | 4 | 89.00 | 59.14 |
13 | 100 | 10 | 10 | 31.59 | 78.88 |
14 | 130 | 13 | 7 | 56.18 | 80.01 |
15 | 100 | 4 | 10 | 29.18 | 74.82 |
16 | 190 | 7 | 7 | 71.15 | 79.84 |
17 | 130 | 7 | 7 | 44.77 | 74.82 |