Table 1.
Data collection and refinement statistics.
| Data collection and processing | IMPα:ACE2 |
|---|---|
| Wavelength (Å) | 0.9537 |
| Resolution range (Å) | 29.98–2.20 (2.27–2.20) |
| Space group | P 21 21 21 |
| Unit cell (Å, o) | 78.94 89.95 100.09 90 90 90 |
| Total reflections | 252,620 (21,940) |
| Unique reflections | 36,873 (3125) |
| Multiplicity | 6.9 (7.0) |
| Completeness (%) | 99.9 (99.8) |
| Mean I/sigma(I) | 15.9 (1.8) |
| Wilson B-factor Å2 | 33.4 |
| R-merge | 0.095 (1.095) |
| R-pim | 0.054 (0.649) |
| CC1/2 | 0.999 (0.807) |
| Refinement | |
| Number of reflections | 36,805 |
| Number of R-free reflections | 1803 |
| R-work (%) | 0.1863 |
| R-free (%) | 0.2099 |
| RMS (bonds) | 0.004 |
| RMS (angles) | 0.67 |
| Ramachandran plot | |
| Favored (%) | 98.83 |
| Allowed (%) | 1.17 |
| Outliers (%) | 0 |
| Average B-factor Å2 | 48.08 |
| Clash score | 2.92 |
| PDB accession code | 7JVO |
Statistics for the highest-resolution shell are shown in parentheses.