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. 2021 May 14;12:440–461. doi: 10.3762/bjnano.12.36

Table 3.

Examples of the polyol process to obtain AgNPs with various morphologies.

[Ag+] EG protector [Ag+]:[Protector] reaction details
(temperature/acid content/time)
AgNP morphology ref.

94 mM 141 mM PVP 1:1.5 EG/140 °C/0.25 mM HNO3 15 h nanocubes
30 nm
[142]
94 mM 147 mM PVP 1:1.5 EG/140 °C/0.025 mM HCl 30 min nanowires
≈30 nm (d)
≈100 nm (c)
[143]
125 mM 188 mM PVP 1:1.5 EG/160 °C 30 min nanocubes
≈80 nm
[139]
250 mM 375 mM PVP 1:1.5 EG/160 °C 45 min nanocubes
≈175 nm
[139]
0.5 mM 0.0625 mM PVP 1:0.0625 PEG/260 °C 24 h nanospheres
≈54 nm
[144]
0.25 M 0.027 M PVP 1:0.108 EG/120 °C 30 min nanospheres
≈27 nm
[145]