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. Author manuscript; available in PMC: 2021 May 26.
Published in final edited form as: ACS Catal. 2020 Feb 10;10(5):3241–3248. doi: 10.1021/acscatal.0c00211

Scheme 6. Derivatization of a Hydrogenated Producta.

Scheme 6.

aConditions: (a) 37% aq. CH2O (1.85 equiv), DCE, 23 °C, 15 min, 93% yield. (b) CDI (4 equiv), THF, 50 °C, 15 h, 84% yield. (c) 40% aq. glyoxal (20 equiv), DCE, 23 °C, 18 h, 41% yield. (d) 60% aq. 2,2-dimethoxyacetaldehyde (1.85 equiv), DCE, 23 °C, 18 h; then Eaton’s Reagent (4 equiv), CH2Cl2, 23 °C, 3 h, 38% yield.