Scope of phenolsa.
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Standard reaction conditions: graphite rod anode, graphite rod cathode, constant current = 10 mA. 2a (0.3–0.4 mmol), 1 (1.5 equiv.), n-Bu4NBF4 (1.0 equiv.), HFIP/CH2Cl2 (6 : 4, 10 mL), rt, 2 h, under N2.
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Standard reaction conditions: graphite rod anode, graphite rod cathode, constant current = 10 mA. 2a (0.3–0.4 mmol), 1 (1.5 equiv.), n-Bu4NBF4 (1.0 equiv.), HFIP/CH2Cl2 (6 : 4, 10 mL), rt, 2 h, under N2.