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. 2020 Mar 20;11(15):3903–3908. doi: 10.1039/d0sc01060j

Construction of the N-dithiophthalimide librarya,b.

graphic file with name d0sc01060j-u1.jpg
a

Reaction conditions: thiol (2 mmol) and N,N′-thiobisphthalimide (3 mmol) in ClCH2CH2Cl (10 mL) were stirred at 80 °C for 2–4 h.

b

Isolated yields.

c

The reaction was performed on a 10 mmol scale.