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(a–d) SEM and
(e–h) TEM images of Cu NCs samples
(a, e) before and (b,f) after potentiostatic electrolysis and pulsed
CO2RR conditions with (c, g) Ean = 0.9 V and (d, h) 1.2 V. Scale bars: (a–d) 100 nm; (e–h)
20 nm.