Table 1.
Crystal data collection and refinement statistics.
| SUN1SBM–SPDYAERD–CDK2 | |
|---|---|
| Data collection | |
|
Wavelength (Å) Space group |
0.91905 C2221 |
| Cell dimensions | |
| a, b, c (Å) | 59.3, 183.5, 103.8 |
| α, β, γ (°) | 90.0, 90.0, 90.0 |
| Resolution (Å) | 3.2 |
| Rmerge (%) | 10.0 (57.3)* |
| I / σI | 13.4 (2.0)* |
| Completeness (%) | 99.3 (94.3)* |
| Redundancy | 5.2 (4.0)* |
| Refinement | |
| Resolution (Å) | 42.59–3.20 |
| No. of reflections | 9095 |
| Rwork/Rfree (%) | 25.2/30.0 |
| No. of atoms | |
|
CDK2 SPDYA |
2396 1216 |
| SUN1 | 166 |
| B-factors (Å2) | |
|
CDK2 SPDYA |
81.5 75.9 |
| SUN1 | 93.4 |
| R.m.s. deviations | |
| Bond lengths (Å) | 0.008 |
|
Bond angles (°) Ramachandran plot (%) Favored region Allowed region Outlier region |
0.040 93.4 100.0 0.0 |
*Highest resolution shell is shown in parenthesis.