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Results of solubility test for poly(tBuAH) samples obtained by CuAAC and HC polymerizations.
| Solvent | Solubility 1 | |
|---|---|---|
| CuAAC | HC 2 | |
| DMSO | ++ | ++ |
| DMF | ++ | ++ |
| THF | ++ | ++ |
| chloroform | ++ | ++ |
| dichloromethane | ++ | ++ |
| acetone | ++ | ++ |
| ethyl acetate | + | + |
| acetonitrile | + | + |
| methanol | – | – |
| water | – | – |
| toluene | – | – |
| diethyl ether | – | – |
1 “++”, “+”, and “–” denote soluble at ≥10 g L−1, soluble at <10 g L−1, and insoluble, respectively. 2 Poly(tBuAH) sample of f1,4 = 0.38.
