Skip to main content
. 2020 Jan 29;11(9):2356–2361. doi: 10.1039/c9sc06265c

Comparison of the parameters used in normal vs. solvent recycling reactions.

Parameters Normal mode Recycling mode
Temperature (°C) 65 65
Flow rate (mL min−1) 0.3 3
Concentration (mM) 10 10
Volume transferred (mL) 3 3
Reaction time (min) 10 10
Valve 1 (reaction solution reservoir) Always on On (0 to 3 min)
Valve 2 (condensation chamber) Always off On (3 to 10 min)