Comparison of the parameters used in normal vs. solvent recycling reactions.
| Parameters | Normal mode | Recycling mode |
|---|---|---|
| Temperature (°C) | 65 | 65 |
| Flow rate (mL min−1) | 0.3 | 3 |
| Concentration (mM) | 10 | 10 |
| Volume transferred (mL) | 3 | 3 |
| Reaction time (min) | 10 | 10 |
| Valve 1 (reaction solution reservoir) | Always on | On (0 to 3 min) |
| Valve 2 (condensation chamber) | Always off | On (3 to 10 min) |