Mass found for each analogue as determined by LC-MS and their respective yields based on resin loading and purity.
Peptide | Mass found | Yield (% purity) |
---|---|---|
9 | 891.5 | 77 (96) |
2 | 1004.6 | 58 (99) |
12 | 994.5 | 30 (98) |
12a | 1094.6 | 10 (97) |
12b | 1108.6 | 5 (99) |
12c | 1192.6 | 1 (97) |
12d | 1122.6 | 3 (99) |
12e | 1142.6 | 1 (99) |
12f | 1198.6 | 6 (99) |
13 | 979.5 | 32 (95) |
13a | 1079.6 | 16 (98) |
13b | 1093.6 | 17 (99) |
13c | 1177.7 | 6 (94) |
13d | 1107.6 | 15 (96) |
13e | 1127.7 | 8 (96) |
13f | 1183.6 | 5 (96) |