Table 3.
Comparison of the catalytic activity of the MCM-41-APS-PMDA-NHSO3H (1) with other catalysts.
| Entry | Catalyst | Amount of catalyst loading | Solvent | Temp. (°C) | Time (min) | Yield (%) | References |
|---|---|---|---|---|---|---|---|
| 1 | PPF-SO3H | 250 mg | EtOH | Reflux | 480 | 81 | 73 |
| 2 | PANI-FeCl3 | 200 mg | CH3CN | Reflux | 1440 | 83 | 82 |
| 3 | Fe3O4/PAA-SO3H | 60 mg | Solvent-free | RT | 120 | 90 | 83 |
| 4 | H2SO4.Silica gel | 30 mol ⁒(47 mg) | Solvent-free | 60 °C | 120 | 89 | 84 |
| 5 | Zr(H2PO4)2 | 7 mol ⁒(20 mg) | Solvent-free | 90 °C | 60 | 92 | 85 |
| 6 | MCM-41-APS-PMDA-NHSO3H | 15 mg | Solvent-free | 80 °C | 35 | 96 | This work |