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. 2021 May 27;11:11199. doi: 10.1038/s41598-021-89572-y

Table 3.

Comparison of the catalytic activity of the MCM-41-APS-PMDA-NHSO3H (1) with other catalysts.

Entry Catalyst Amount of catalyst loading Solvent Temp. (°C) Time (min) Yield (%) References
1 PPF-SO3H 250 mg EtOH Reflux 480 81 73
2 PANI-FeCl3 200 mg CH3CN Reflux 1440 83 82
3 Fe3O4/PAA-SO3H 60 mg Solvent-free RT 120 90 83
4 H2SO4.Silica gel 30 mol ⁒(47 mg) Solvent-free 60 °C 120 89 84
5 Zr(H2PO4)2 7 mol ⁒(20 mg) Solvent-free 90 °C 60 92 85
6 MCM-41-APS-PMDA-NHSO3H 15 mg Solvent-free 80 °C 35 96 This work