Sample | 1Pt·0.5MeOH | 1Pd·0.5MeOH | ||||||
T (K) | 260 | 100 | 260 | 100 | ||||
Fe1(HS) | Fe2(HS) | Fe1(HS) | Fe2(LS) | Fe1(HS) | Fe2(HS) | Fe1(HS) | Fe2(LS) | |
Fe–N (Å) | 2.174 | 2.166 | 2.164 | 1.984 | 2.174 | 2.173 | 2.155 | 1.986 |
Θ/Σ | 29/4.7 | 28/19.7 | 37/17.6 | 26/9.7 | 32/8.4 | 28/22.4 | 32/18.0 | 25/11.9 |