Entry | Catalyst | % yielda |
---|---|---|
1 | 1 | 86 ± 5 (13 h) |
2 | 2 | 35 (13 h) |
Yields are mean ± standard deviation of measurements performed at least in duplicate. Reactions were run on a 0.05 mmol scale. Product yields were determined by 1H NMR using mesitylene as an internal standard.
For the oxidative coupling of benzylamine, ESI-MS was further used to confirm the presence of the desired product ([M + H]+m/z = 256.09).