Table 1. Solubility Screening.
solubility (mg/mL) | ||||||
---|---|---|---|---|---|---|
compound-6 |
TPPO-H2DIAD |
TPPO |
||||
solvent | RT | 0 °C | RT | 0 °C | RT | 0 °C |
2-propanol | insoluble | insoluble | 60.4 | 13.3 | 46.5 | 25.4 |
tetrahydrofuran | 124.5 | 101.0 | 157.5 | 61.0 | 169.7 | 105.0 |
cyclohexane | insoluble | insoluble | insoluble | insoluble | insoluble | insoluble |
toluene | 46.7 | 42.1 | 23.2 | 15.95 | 44.3 | 42.9 |