Table 3. Quantitative % Content (w/w) of Compound-6 and TPPO by HPLC.
| % content (w/w) | compound-6 | TPPO |
|---|---|---|
| reaction mixture | 20.55 | 29.33 |
| TPPO- H2DIAD | 0.14 | |
| toluene residue | 24.86 | 6.25 |
| pure compound-6 | 0.05 | |
| IPA residue | 13.21 | 10.97 |
| % content (w/w) | compound-6 | TPPO |
|---|---|---|
| reaction mixture | 20.55 | 29.33 |
| TPPO- H2DIAD | 0.14 | |
| toluene residue | 24.86 | 6.25 |
| pure compound-6 | 0.05 | |
| IPA residue | 13.21 | 10.97 |