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. 2021 May 19;6(21):13940–13945. doi: 10.1021/acsomega.1c01996

Table 3. Quantitative % Content (w/w) of Compound-6 and TPPO by HPLC.

% content (w/w) compound-6 TPPO
reaction mixture 20.55 29.33
TPPO- H2DIAD 0.14  
toluene residue 24.86 6.25
pure compound-6   0.05
IPA residue 13.21 10.97