Table 2.
Isolated yield. Absolute configuration assigned by analogy to that of 1g, which was determined to be (S) by single-crystal X-ray diffraction.
Selectivity factor (s) was calculated according ln[(1-C)(1 eeSM)/1-C](1+eeSM)]. For isolated yields of kinetic resolution, see Supporting Information.
5.0 mol% of catalyst was used.
Reaction time variation: 12 h.
Reaction time variation: 18 h.
Reaction time variation: 20 h.