Fig. 2. Electrochemical, spectroelectrochemical and photoelectrochemical properties of csiMOF-6 probed by (a) CV, (b) solid state UV-Vis-NIR SEC, and (c) solid state EPR SEC at −1.3 V vs. Fc/Fc+. Spectral colours: black = starting spectrum; grey = spectral progression showing electrochemical generation of the radical monoanion; red = maximum of the spectral reduction; and green = photoexcited radical generated upon in situ light irradiation in the UV-Vis-NIR SEC cell. Arrows indicate sweep direction or spectral changes.
