Ball milling method |
Facile; highly effective; economic; scalable |
Products with uneven and large size; generation of noise |
[33, 40, 45, 48, 250] |
Hydrothermal/solvothermal method |
Facile morphological control; controllable size; high purity |
High cost; simple morphology; difficult controlled processes; existing safety problems |
[38, 46, 61, 62, 99, 106, 157, 199] |
Solution method |
Well-controlled size; uniform dispersion |
Related toxic reagent |
[47, 63, 95, 165, 214, 251, 252] |
Vaporization–condensation method |
Uniform and small size; controllable nanostructure |
Difficult controlled distribution; low production efficiency |
[50, 122, 217, 253] |
Calcination/carbothermic reduction |
Well operability; generation of new phases |
Large energy consumption; generation of toxic gases |
[44, 53–55, 57, 80, 81, 89, 96–98, 100–102, 104, 105, 128, 129, 131, 132, 135, 198, 202] |
Electrodeposition method |
Uniform size; controllable |
Related toxic reagent; large energy consumption |
[49] |
Solid–liquid reaction method |
Simple; facile operability |
Related dangerous solution and toxic reagent |
[52, 60, 103, 254–256] |
Chemical vapor deposition method |
Precise controlled products; high purity |
Required relatively high deposition temperatures; involving some dangerous precursors; large energy consumption |
[127, 257] |