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RAFT polymerization and post-polymerization conjugation allows for facile and precise control of DMA-co-TEMPO copolymer synthesis. (A) Two-step synthesis scheme of polymers by (1) RAFT polymerization of DMA and PFPA and (2) post-polymerization substitution of TEMPO-amine for PFPA. (B) 19F NMR confirming removal of PFPA units on the final polymer.
