Table 1.
Run | Catalyst | Catalyst/OLLA (wt%) | Temperature (°C) | Time (h) | Pressure (torr) | MW (g/mol) | Yield (%) |
---|---|---|---|---|---|---|---|
1 | GeO2 | 0.8 | 180 | 20 | 10 | 28,000 | 73 |
2 | Sb2O3 | 0.1 | 200 | 30 | 20 | 20,000 | 25 |
3 | ZnO | 0.1 | 200 | 30 | 20 | 36,000 | 35 |
4 | Fe2O3 | 0.1 | 200 | 8 | 1 | 20,000 | 23 |
5 | Al2O3 | 8.5 | 200 | 30 | 20 | 27,000 | 42 |
6 | SiO2 | 0.8 | 180 | 20 | 10 | 11,000 | 58 |
7 | TiO2 | 0.8 | 180 | 20 | 10 | 11,000 | 64 |
8 | SnO | 0.2 | 180 | 20 | 10 | 50,000 | 36 |
9 | SnCl2·2H2O | 0.4 | 180 | 20 | 10 | 41,000 | 43 |
10 | TSA | 0.34 | 180 | 10 | 10 | 17,000 | 70 |