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. 2021 May 31;13(11):1822. doi: 10.3390/polym13111822

Table 1.

Typical results of the catalyst screening test for the melt polycondensation of OLLA Reprinted with permission from ref. [40]. Copyright 2000 John Wiley & Sons, Inc.

Run Catalyst Catalyst/OLLA (wt%) Temperature (°C) Time (h) Pressure (torr) MW (g/mol) Yield (%)
1 GeO2 0.8 180 20 10 28,000 73
2 Sb2O3 0.1 200 30 20 20,000 25
3 ZnO 0.1 200 30 20 36,000 35
4 Fe2O3 0.1 200 8 1 20,000 23
5 Al2O3 8.5 200 30 20 27,000 42
6 SiO2 0.8 180 20 10 11,000 58
7 TiO2 0.8 180 20 10 11,000 64
8 SnO 0.2 180 20 10 50,000 36
9 SnCl2·2H2O 0.4 180 20 10 41,000 43
10 TSA 0.34 180 10 10 17,000 70